This submission belongs to the session a. General Organic Synthesis of the event The 12th International Electronic Conference on Synthetic Organic Chemistry
Published date
13 Nov, 2008
Citation
Azadeh Tadjarodi, Neda Imani, Solvent-free synthesis of Pyridine-2-aminium-6-methyl Pyridine-2,6-dicarboxylate under ball-milling conditions, in Proceedings of The 12th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2008, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-12-01223
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Solvent-free synthesis of Pyridine-2-aminium-6-methyl Pyridine-2,6-dicarboxylate under ball-milling conditions
Azadeh Tadjarodi 1
Neda Imani 1
1. Physical chemistry laboratory, Chemistry Faculty, Iran University of Science and Technology
Abstract
A novel proton transfer compound, pyridine-2-aminium-6-methyl pyridine-2,6-dicarboxylate, has been synthesized by the reaction between 2,6-pyridinedicarboxylic acid, [pydc,H2], and 2-amino-6-methyl- pyridine, [pya], in 1:1 molar ratio under ball milling conditions. The title compound has been characterized by spectral methods (1H-, 13CNMR, IR).
Keywords
Solvent free
Pyridine-2,6-dicarboxylic acid
Proton transfer
Ball milling
Ion pairs
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