EventsThe 11th International Electronic Conference on Synthetic Organic Chemistry
Event submissions
Published
with-doi10.3390/ecsoc-11-01352
This submission belongs to the session e. Symposium on Microwave Assisted Synthesis of the event The 11th International Electronic Conference on Synthetic Organic Chemistry
Published date
30 Nov, 2007
Citation
Ellis Benjamin, Yousef Hijji, A Novel Microwave Synthesis of Unsubstituted Cyclic Imides, in Proceedings of The 11th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2007, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-11-01352
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A Novel Microwave Synthesis of Unsubstituted Cyclic Imides

Ellis Benjamin 1
Yousef Hijji 2
1. Department of Chemistry and Physics, Arkansas State University, AR 72467, USA
2. Department of Chemistry, Morgan State University, Baltimore, MD 21251, USA
Abstract
A number of unsubstituted cyclic imides were synthesized from cyclic anhydrides, hydroxylamine hydrochloride NH 2 OH (HCl), and 4-N,N-dimethylaminopyridine (DMAP) under microwave irradiation in a mono-mode microwave. This synthesis gave the unsubstituted cyclic imides in high yields (61-81%) instead of the predicted N-hydroxy cyclic imides which were found to be the minor products.
Keywords
Hydroxylamine (HCl)
Unsubstituted Cyclic Imides
DMAP
Microwave
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