EventsThe 10th International Electronic Conference on Synthetic Organic Chemistry
Event submissions
Published
with-doi10.3390/ecsoc-10-01442
This submission belongs to the session e. Symposium on Microwave Assisted Synthesis of the event The 10th International Electronic Conference on Synthetic Organic Chemistry
Published date
30 Nov, 2006
Citation
Julio A. Seijas, M. Pilar Vázquez-Tato, José Crecente-Campo, Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves, in Proceedings of The 10th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2006, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-10-01442
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Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves

Julio A. Seijas 1
M. Pilar Vázquez-Tato 1
José Crecente-Campo 1
1. Departamento de Química Orgánica. Facultad de Ciencias. Universidad de Santiago de Compostela. Aptdo. 27080-Lugo. Spain
Abstract
Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes.
Keywords
n/a
Microwave assisted oxidation reaction on polyaniline containing heterogeneous catalysts
Host-Guest Dynamics studied by Fluorescence Correlation Spectroscopy