EventsThe 9th International Electronic Conference on Synthetic Organic Chemistry
Event submissions
Published
with-doi10.3390/ecsoc-9-01641
This submission belongs to the session e. Symposium on Microwave Assisted Synthesis of the event The 9th International Electronic Conference on Synthetic Organic Chemistry
Published date
01 Nov, 2005
Citation
Vladimir N. Bulavka, Note to Titanium (III) and (IV) Phthalocyanines Synthesis in Modified Microwave Oven, in Proceedings of The 9th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2005, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-9-01641
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Note to Titanium (III) and (IV) Phthalocyanines Synthesis in Modified Microwave Oven

Vladimir N. Bulavka 1
1. Slavich Company, Mendeleev sq. 2, Pereslavl-Zalesskiy, Yaroslavl region 152020, Russian Federation
Abstract
Microwave irradiation of 1,2-dicyanobenzene (phthalodinitrile) and reducing agent (hydrogen donor) or 1,3-diiminoisoindoline in organic solvents with titanium (III) or titanium (IV) chlorides after treating with water leads to titaniumoxo (IV) phthalocyanine. The formation of titaniumchloro (III) phthalocyanine in solvent-free conditions and in solvents under microwave irradiation is discussed.
Keywords
mmicrowaves
titaniumchloro (III) phthalocyanine
titaniumdichloro (IV) phthalocyanine
titaniumoxo (IV) phthalocyanine
Microwave-Assisted Oxidation of Starch Using Hydrogen Peroxide
P2S5 Mediated Synthesis of Benzoxazoles and Benzothiazoles by Microwave Irradiation