Events The 9th International Electronic Conference on Synthetic Organic Chemistry

Event submissions

Published

This submission belongs to the session e. Symposium on Microwave Assisted Synthesis of the event The 9th International Electronic Conference on Synthetic Organic Chemistry

Published date

01 Nov, 2005

Citation

Ewa Wolff, Dariusz Bogdal, André Loupy, Michel Bortolussi, Microwave-Assisted Synthesis of Polyesters Containing 1,4:3,6-dianhydrohexitols, in Proceedings of The 9th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2005, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-9-01644

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Microwave-Assisted Synthesis of Polyesters Containing 1,4:3,6-dianhydrohexitols

Ewa Wolff ¹

Dariusz Bogdal ¹

André Loupy ²

Michel Bortolussi ²

1. Departament of Chemistry, Politechnika Krakowska, ul. Warszawska 24, 31-155 Krakow, Poland

2. Laboratoire des Réactions Sélectives sur Supports, ICMMO, CNRS UMR 8615, Université Paris–Sud, Bâtiment 410, 91405 Orsay Cedex, France

Abstract

Series of reactions were carried out for three dianhydrohexitols (isosorbide, isomannide and isoidide) and one aliphatic carboxylic acid – suberic acid - and its derivatives. The reactions were performed in the microwave reactor in an open vessel equipped with mechanical stirrer. Polymer products with highest yields were obtained in reaction of isosorbide and suberoyl chloride. For microwave reactions with the most satisfactory yields, conventional synthesis were also performed.

Keywords

polyesters

dianhydrohexitols

microwave

Microwave Assisted Organic Synthesis of Benzamides with C3 Symmetry

Microwave Inducted Thermal Gradients in Solventless Reaction Systems