This submission belongs to the session a. General Organic Synthesis of the event The 13th International Electronic Conference on Synthetic Organic Chemistry
Published date
31 Oct, 2009
Citation
M. J. Rodríguez-Doutón, Marcelino Maneiro, A. M. Gonzalez-Noya, B. Fernández, M. I. Fernández-García, M. A. Vázquez- Fernández, CRYSTAL STRUCTURE OF (N-N'-BIS(3-ETHOXYSALICYLIDENE)-1,2-DIAMINOPROPANE, in Proceedings of The 13th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2009, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-13-00183
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CRYSTAL STRUCTURE OF (N-N'-BIS(3-ETHOXYSALICYLIDENE)-1,2-DIAMINOPROPANE
M. J. Rodríguez-Doutón 1
Marcelino Maneiro 1
A. M. Gonzalez-Noya 1
B. Fernández 1
M. I. Fernández-García 1
M. A. Vázquez- Fernández 1
1. Dpto. de Química Inorgánica. Facultad de Ciencias. Univ. de Santiago de Compostela, Lugo 27002, Spain
Abstract
Three hexadentate Schiff base ligands were obtained by condensation of 3-ethoxy-2-hydroxybenzaldehyde and different diamines (1,2-diaminoethane, 1,2-diaminopropane, 1,2-diamino-2-metylpropane) to yield H2Ln (H2L1, H2L2 and H2L3, respectively). The ligands have been characterised by elemental analysis, IR, and 1H and 13C NMR spectroscopic techniques, mass spectrometry (ES) and X-ray diffraction.
Keywords
SYNTHESIS OF HIGHLY FUNCTIONALIZED NON-RACEMIC CHIRAL ALKYL HALIDES USING KHARASCH ADDITION
N-Alkyl-N-[5-(propylamino)-9H-benzo[a]phenoxazin-9-ylidene]alkan-1- aminium chlorides: synthesis and photophysical studies