This submission belongs to the session a. General Organic Synthesis of the event The 1st International Electronic Conference on Synthetic Organic Chemistry
Published date
01 Sep, 1997
Citation
Vasile Surducan, Emanoil Surducan, Gabriela Nagy, Sorin V. Filip, Microwave Application in Organic Synthesis. Microwave-Assisted Preparation of Diphenylamines in 'Dry Media', in Proceedings of The 1st International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 1997, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-1-02028
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Microwave Application in Organic Synthesis. Microwave-Assisted Preparation of Diphenylamines in 'Dry Media'
Sorin V. Filip 1
Gabriela Nagy 1
Emanoil Surducan 1
Vasile Surducan 1
1. Institute for Isotopic and Molecular Technology, P.O.Box 700, Cluj-Napoca 5,
RO-3400, Romania
Abstract
The application of microwaves in organic chemistry has experienced exponential growth within the last eight years. Rate enhancements varied from 10 to 1500 times compared with those of conventionally heated samples. We propose here a new technology for preparation of diphenylamine by microwave-activation, using an inorganic solid support, namely bentonite. This method offers the following advantages over conventional synthesis of this compound: high efficiency, safety, the experimental procedure is much simpler and environmental friendly.
Keywords
Microwave
organic synthesis
dyphenilamine
solid support
bentonite
environment.
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