Events The 18th International Electronic Conference on Synthetic Organic Chemistry

Event submissions

Published

This submission belongs to the session c. Microwave Assisted Synthesis of the event The 18th International Electronic Conference on Synthetic Organic Chemistry

Published date

03 Nov, 2014

Citation

Julio A. Seijas, Alberto Diaz-Seivane, María García-Fernández, M. Pilar Vázquez-Tato, Microwave Assisted Synthesis of Tripodal Tris(1H-1,2,3-triazol-4-yl) Cyanurates and Melamines, in Proceedings of The 18th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2014, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-18-c013

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Microwave Assisted Synthesis of Tripodal Tris(1H-1,2,3-triazol-4-yl) Cyanurates and Melamines

Julio A. Seijas ¹

Alberto Diaz-Seivane ¹

María García-Fernández ¹

M. Pilar Vázquez-Tato ¹

1. Departamento de Química Orgánica. Facultade de Ciencias. Universidade de Santiago de Compostela. Campus Terra. 27080-Lugo. Spain

Abstract

2,4,6-tris(prop-2-yn-1-yloxy)-1,3,5-triazine and N2,N4,N6-tri(prop-2-yn-1-yl)-1,3,5-triazine-2,4,6-triamine are used in click reactions to prepare tripodal compounds and dendrimer cores. So, 1,3-cycloaddition with benzyl azide under microwave irradiation afforded 2,4,6-tris((1-benzyl-1H-1,2,3-triazol-4-yl)methoxy)-1,3,5-triazine and N²,N⁴,N⁶-tris((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-1,3,5-triazine-2,4,6-triamine, in a 1 minute reaction with good yields.

Keywords

Triazole

triazine

tripodal

dendrimer

microwave

Manuscript

jasvecsoc18pilarjasvfinal.pdf

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