EventsThe 5th International Electronic Conference on Processes
Published
This submission belongs to the session S5. Materials Manufacturing and Sustainable Packaging of the event The 5th International Electronic Conference on Processes
Published date
15 Oct, 2026
Academic Editor
author-avatarBlaž Likozar
Citation
Paulo Henrique Eleuterio Falsetti, Letícia Vieira Savazi, Douglas Mendes da Silva del Duque, Jéssica Cristina de Almeida, Maria Fernanda de Almeida Freitas, Milena Vitória de Campos Chagas, Vinícius Bertolini Montoni, Alexandre Drezza Menezes, Wilton Moreira Ferraz Junior, Caue Ribeiro de Oliveira, Guillermo Díaz-Sainz, Vagner Romito de Mendonça, IFSpray Coater: Development and Validation of a Low-Cost Open-Source Spray Coating Platform for Gas Diffusion Electrode Fabrication Using a Repurposed 3D Printer, in Proceedings of The 5th International Electronic Conference on Processes, 20 October–22 October 2026, MDPI: Basel, Switzerland
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IFSpray Coater: Development and Validation of a Low-Cost Open-Source Spray Coating Platform for Gas Diffusion Electrode Fabrication Using a Repurposed 3D Printer

Letícia Vieira Savazi 2
Maria Fernanda de Almeida Freitas 3
Milena Vitória de Campos Chagas 3
Vinícius Bertolini Montoni 3
Alexandre Drezza Menezes 3
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1. Center for Science and Technology for Sustainability, Federal University of São Carlos - Sorocaba - São Paulo - Brazil
2. Graduate Program in Materials Science, Federal University of São Carlos - Sorocaba - São Paulo - Brazil
3. Federal Institute of Education, Science and Technology of São Paulo - Itapetininga - São Paulo - Brazil
4. Embrapa Instrumentation- São Carlos - SP - Brazil
5. Chemical and Biomolecular Engineering Department - University of Cantabria - Santander - Cantabria - Spain
Abstract

Automation has become increasingly important in laboratory environments, enhancing reproducibility, precision, and efficiency while reducing operator-dependent variability. In materials processing, where small deviations in experimental parameters can strongly affect final properties, automated systems enable tighter control and systematic exploration of process variables. This is particularly relevant for the fabrication of functional electrochemical materials such as gas diffusion electrodes (GDEs), where coating uniformity and thickness directly influence performance in CO2 electrochemical reduction (CO2ER) systems. Low-cost and open-source approaches based on repurposed equipment therefore provide accessible alternatives for expanding experimental capabilities in research laboratories. This work aims to develop and experimentally validate a low-cost spray coater, named IFSpray Coater, based on a 3D printer platform for thin-film deposition in GDE fabrication. The system was built from a modified Ender-3 Pro architecture, combining planar motion with a fixed pneumatic spray unit. Trajectory generation was performed using the open-source software 2D SprayPath (PauloFalsetti/2D_SprayPath), enabling parameterized control of x–y scanning patterns. Nozzle height, safety distance, and bed configuration were optimized to ensure stable spray formation and reproducible coatings. A zig-zag scanning strategy was employed, with defined scan area, step size, velocity, and number of repetitions. System performance was assessed by comparing nominal and measured deposition parameters. Results showed strong agreement, with relative errors below 1% for most spatial variables. Scan area deviations remained below 1%, while step size showed slightly higher variation (up to 1.5%) due to mechanical tolerances and motion resolution limits. Spray width remained stable at 3.2 ± 0.5 mm. Two configurations were evaluated (100 × 100 mm2 and 60 × 60 mm2), with the latter improving overlap and coating homogeneity. Experimental patterns closely matched simulated trajectories, confirming reliable translation from design to deposition. Overall, the system demonstrated high accuracy and repeatability, supporting low-cost fabrication of GDEs for CO2 electroreduction systems.

Keywords
Spray coating
Gas diffusion electrodes
Laboratory automation
Open-source hardware
Thin-film deposition
3D printer
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