EventsThe 14th International Electronic Conference on Synthetic Organic Chemistry
Event submissions
Published
with-doi10.3390/ecsoc-14-00451
This submission belongs to the session c. Microwave Assisted Synthesis of the event The 14th International Electronic Conference on Synthetic Organic Chemistry
Published date
30 Oct, 2010
Citation
Hoang Thi Kim Van, Nguyen Dinh Thanh, REACTION OF ACETOPHENONE (HEPTA-O-ACETYL-b-LACTOSYL)THIOSEMICARBAZONES WITH ETHYL BROMOACETATE, in Proceedings of The 14th International Electronic Conference on Synthetic Organic Chemistry, 1 November–30 November 2010, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-14-00451
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REACTION OF ACETOPHENONE (HEPTA-O-ACETYL-b-LACTOSYL)THIOSEMICARBAZONES WITH ETHYL BROMOACETATE

Hoang Thi Kim Van
Nguyen Dinh Thanh
Abstract
Reaction of substituted acetophenone (hepta-O-acetyl-b-lactosyl)thiosemicarbazones with ethyl bromoacetate was performed in the presence of anhydrous sodium acetate using microwave-assisted heating method. The reaction yields were 64-80%. Structure of 2-iminothiazolidin-4-one products was confirmed by spectroscopic methods. Isomer ratios 2 and 2' were determined by 1H NMR.
Keywords
SYNTHESIS OF SOME (HEPTA-O-ACETYL-b-LACTOSYL)THIOSEMICARBAZONES CONTAINING BENZENE RING
STUDY ON REACTION OF ETHYL BROMOACETATE WITH SOME (HEPTA-O-ACETYL-b-MALTOSYL)THIOSEMICARBAZONES OF SUBSTITUTED ACETOPHENONES