Events The 24th International Electronic Conference on Synthetic Organic Chemistry

Event submissions

Published

This submission belongs to the session A. General Organic Synthesis of the event The 24th International Electronic Conference on Synthetic Organic Chemistry

Published date

14 Nov, 2020

Citation

Erick Cuevas-Yañez, Raul E. Raul Gordillo-Cruz, Liliana Gonzalez-Reyes, Milton Coporo-Reyes, Nieves Zavala-Segovia, Bernardo A. Frontana-Uribe, Marco A. García-Eleno, M. V. Basavanag Unnamatla, Microwave-assisted Asinger synthesis of thiazolines, in Proceedings of The 24th International Electronic Conference on Synthetic Organic Chemistry, 15 November–15 December 2020, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-24-08316

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Microwave-assisted Asinger synthesis of thiazolines

Raul E. Raul Gordillo-Cruz ¹

Liliana Gonzalez-Reyes ¹

Milton Coporo-Reyes ¹

Nieves Zavala-Segovia ¹

Bernardo A. Frontana-Uribe ¹

Marco A. García-Eleno ¹

M. V. Basavanag Unnamatla ¹

Erick Cuevas-Yañez ^1,2

1. Centro Conjunto de Investigación en Química Sustentable UAEM-UNAM, Carretera Toluca-Atlacomulco Km. 14.5, Toluca, Estado de México 50200, Mexico

2. Facultad de Química, Facultad de Química, Universidad Autónoma del Estado de México. Paseo Colón esq. Paseo Tollocan, 50120, Toluca, Mexico

Abstract

An array of 2,4-disubstituted thiazolines was obtained through Asinger reaction approach from the straightforward treatment of diverse aldehydes/ketones with 1-mercaptopropan-2-one in presence of NH3 assisted by microwave irradiation displaying similar and sometimes higher yields as well as shorter reaction times that traditional Asinger rection conditions at room and lower temperatures.

Keywords

thiazoline

Asinger Reaction

microwave irradiation

Manuscript

sciforum-039159.pdf

On the acylation of 1,6-diamino-2-oxo-1,2-dihydropyridine-3,5-dicarbonitriles

Synthesis of conjugated polymer based in Zn(II) porphyrin bearing terminal alkynyl groups as photosensitizer