Events The 24th International Electronic Conference on Synthetic Organic Chemistry

Event submissions

Published

This submission belongs to the session C. Microwave Assisted Synthesis of the event The 24th International Electronic Conference on Synthetic Organic Chemistry

Published date

14 Nov, 2020

Citation

Azadeh Tadjarodi, Mahdi Bahmani, Mina Imani, Facile microwave-assisted synthesis of heterostructured CuCo₂S₄/CuCo₂O₄ nanoparticles using organic agent of thiourea, in Proceedings of The 24th International Electronic Conference on Synthetic Organic Chemistry, 15 November–15 December 2020, MDPI: Basel, Switzerland, doi: 10.3390/ecsoc-24-08347

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Facile microwave-assisted synthesis of heterostructuredCuCo₂S₄/CuCo₂O₄ nanoparticles using organic agent of thiourea

Mahdi Bahmani ¹

Mina Imani ¹

Azadeh Tadjarodi ²

1. Research Laboratory of Inorganic Materials Synthesis, Department of Chemistry, Iran University of Science and Technology, 16846-13114 Tehran, Iran

2. Research Laboratory of Inorganic Materials Synthesis, Department of Chemistry, Iran University of Science and Technology, Narmak, Tehran, Iran

Abstract

Ultra-fast one-put microwave assisted strategy is introduced for the synthesis of heterostructured CuCo₂S₄/CuCo₂O₄ nanoparticles into a domestic microwave oven with the power of 900 W for 20 minutes. Thiourea as an organic agent was used as a sulfur source and driving agent to lead the solvent free combustion reaction to obtain this earth-abundant and low-cost mixed chalcogenide/oxide product. The structural and morphological specifications were studied in details using powder x-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM) and energy dispersion of x-ray spectrometry (EDX). The employed strategy relatively clarifies a new facile, rapid and eco-friendly route to produce heterostructured nanocomposites for different functional purposes. The electrochemical properties of the prepared product as an electrode material in energy storage applications was studied in details.

Keywords

Microwave

Nanoparticles

Thiourea

Chalcogenide

Manuscript

MicrowaveAssistedSynthesis_8347 - done.pdf

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Facile microwave-assisted synthesis of heterostructuredCuCo₂S₄/CuCo₂O₄ nanoparticles using organic agent of thiourea