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Microwave-assisted solvent-free synthesis of Thiocarbamic acid [(thiophene-2-yl) ethylidene]hydrazide
Published:
31 October 2009
by MDPI
in The 13th International Electronic Conference on Synthetic Organic Chemistry
session Symposium on Microwave Assisted Synthesis
Abstract: A fast and efficient method has been developed for the synthesis of Thiocarbamic acid [(thiophene-2-yl) ethylidene]hydrazide, [TTEH], under microwave irradiation. This compound has been characterized by FT-IR, 1H-NMR, 13C-NMR.
Keywords: thiosemicarbazide; microwave; 2-acetylthiophene; solvent free