Crystal structure of H4L1 (N-N’-Bis(o-hydroxybenzoyl)ethylenediamine)

M. Vázquez-Fernández; M. Fernández; B. Fernández; A. González-Noya; M. Rodríguez-Doutón

doi:10.3390/ecsoc-10-01413

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Synthesis and characterization of new Mannich base ligand. Structure of N, N-bis-(4,5-dimethyl-2-hydroxybenzyl)-N(2-pyridylmethyl)amine

Crystal structure of H4L1 (N-N’-Bis(o-hydroxybenzoyl)ethylenediamine)

M. A. Vázquez-Fernández

M. I. Fernández

^*,

B. Fernández

A. M. González-Noya

M. J. Rodríguez-Doutón

¹ Dpto. de Química Inorgánica. Facultad de Ciencias. Univ. de Santiago de Compostela. Lugo 27002, Spain

Published: 30 November 2006 by MDPI in The 10th International Electronic Conference on Synthetic Organic Chemistry session General Organic Synthesis

https://doi.org/10.3390/ecsoc-10-01413

Abstract: Three bis-amide bis-phenoxy N2O2 ligands were obtained from the 2:1 molar reaction of phenyl salicylate and the diamines (1,2-diaminoethane, 1,3-diaminopropane and 1,4-diaminobutane) to yield H4Ln (H4L1, H4L2, H4L3 respectively). The ligands have been characterised by elemental analysis, IR, and 1H 13C NMR spectroscopies, mass spectrometry (ES) and X-ray diffraction.

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M. Vázquez-Fernández

M. Fernández

B. Fernández

A. González-Noya

M. Rodríguez-Doutón