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Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves
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1  Departamento de Química Orgánica. Facultad de Ciencias. Universidad de Santiago de Compostela. Aptdo. 27080-Lugo. Spain

Abstract: Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes.
Keywords: n/a