Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves

Julio Seijas; M. Vázquez-Tato; José Crecente-Campo

doi:10.3390/ecsoc-10-01442

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Host-Guest Dynamics studied by Fluorescence Correlation Spectroscopy

Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves

Julio A. Seijas

^*,

M. Pilar Vázquez-Tato

^*,

José Crecente-Campo

¹ Departamento de Química Orgánica. Facultad de Ciencias. Universidad de Santiago de Compostela. Aptdo. 27080-Lugo. Spain

Published: 30 November 2006 by MDPI in The 10th International Electronic Conference on Synthetic Organic Chemistry session Symposium on Microwave Assisted Synthesis

https://doi.org/10.3390/ecsoc-10-01442

Abstract: Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes.

Keywords: n/a

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Julio Seijas

M. Vázquez-Tato

José Crecente-Campo