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Synthesis of Pentachlorofluororhenate (V) with Tetramethylammonium Counter Ion, by New a Method
* 1, 2 , 3
1  Faculty of Science, Islamic Azad University. Science and research branch, Tehran , Iran
2  Faculty of Science, Islamic Azad University, Firoozabad Branch, Iran
3  Department of Chemistry, Faculty of Science, Imam Khomeini International University, Qazvin, Iran

Abstract: A new, simple and one-step method used for synthesis of new compound tetramethylammonium pentachlorofluororhenate- (V) in very high yield. This compound one of the mixed halo complexes of rhenium that have been prepared by the reaction between tetramethylammonium fluoride and ReCl5 in 1:1 molar ratio in the minimum amount of dry acetonitrile. The compound has been characterized by elemental analyses and IR spectral studies.
Keywords: n/a