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Synthesis of Pentachlorofluororhenate (V) with Tetramethylammonium Counter Ion, by New a Method
Published: 30 November 2007 by MDPI in The 11th International Electronic Conference on Synthetic Organic Chemistry session General Organic Synthesis
Abstract: A new, simple and one-step method used for synthesis of new compound tetramethylammonium pentachlorofluororhenate- (V) in very high yield. This compound one of the mixed halo complexes of rhenium that have been prepared by the reaction between tetramethylammonium fluoride and ReCl5 in 1:1 molar ratio in the minimum amount of dry acetonitrile. The compound has been characterized by elemental analyses and IR spectral studies.