Facile Synthesis of 1,1-Diacetates Catalyzed by MCM-41-SO3H Under Solvent-free Condition

Mohammad Ghorban Dekamin; Hesam Tourani; Mohammad Reza Naimi-Jamal

doi:10.3390/ecsoc-15-00768

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Nano-Ordered MCM-41-SO3H as a Heterogeneous and Efficient Catalyst for Synthesis of Bis(indolyl)methanes Under Solvent-Free Conditions

Facile Synthesis of 1,1-Diacetates Catalyzed by MCM-41-SO3H Under Solvent-free Condition

Mohammad Ghorban Dekamin

Hesam Tourani

Mohammad Reza Naimi-Jamal

¹ Department of Chemsitry, Iran University of Science and Technology, Tehran, Iran

Published: 02 November 2011 by MDPI in The 15th International Electronic Conference on Synthetic Organic Chemistry session General Organic Synthesis

https://doi.org/10.3390/ecsoc-15-00768

Abstract: We report herein that acylals can be prepared very fast and in excellent yields by the direct condensation of aldehydes with acetic anhydride under solvent-free condition by employing of a mesoporous derivatized Mobile Crystalline Material, MCM-41-SO₃H as heterogeneous catalyst at room temperature.

Keywords: Acylals, MCM Mesoporous Materials, Carbonyl Protection

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Mohammad Ghorban Dekamin

Hesam Tourani

Mohammad Reza Naimi-Jamal