Tetrabutylammonium phtalimide-N-oxyl (TBAPINO) as an efficient, safe and recoverable catalyst for rapid trimethylsilyl protection of hydroxyl groups

Mohammad Dekamin; Javad Mokhtari; M. Naimi-Jamal

doi:10.3390/ecsoc-12-01235

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Tetrabutylammonium phtalimide-N-oxyl (TBAPINO) as an efficient, safe and recoverable catalyst for rapid trimethylsilyl protection of hydroxyl groups

Mohammad G. Dekamin

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Javad Mokhtari

M. Reza Naimi-Jamal

¹ College of Chemistry, Iran University of Science and Technology, Tehran, 16846-13114, Iran

Published: 01 November 2008 by MDPI in The 12th International Electronic Conference on Synthetic Organic Chemistry session General Organic Synthesis

https://doi.org/10.3390/ecsoc-12-01235

Abstract: Tetrabutylammonium phtalimide-N-oxyl (TBAPINO) can be used as an efficient organocatalyst for the conversion of alcohols to their corresponding trimethylsilyl ethers with hexamethyldisilazane (HMDS). All reactions were performed under mild and completely homoogeneous reaction conditions in high to quantitative yields.

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Mohammad Dekamin

Javad Mokhtari

M. Naimi-Jamal