Microwave synthesis of [6-Diethylamino-9-(2-octylcarbamoyl-phenyl)-xanthen-3-ylidene]-diethyl-amine and its isomer

Ellis Benjamin; Earl Benjamin; Evan Pannkuk

doi:10.3390/ecsoc-14-00463

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Microwave synthesis of [6-Diethylamino-9-(2-octylcarbamoyl-phenyl)-xanthen-3-ylidene]-diethyl-amine and its isomer

Ellis Benjamin

^{*

1, 2},

Earl Benjamin

^{1, 2},

Evan Pannkuk

^{1, 3}

¹ Department of Chemistry and Physics, Arkansas State University, PO Box 419, State University, AR, 72467, USA
² The Applied and Synthetic Laboratory, Arkansas, State University, PO Box 419, State University, AR, 72467 USA
³ Graduate Program in Environmental Sciences, PO Box 847, Arkansas State University, State University, AR, 72467, USA

Published: 30 October 2010 by MDPI in The 14th International Electronic Conference on Synthetic Organic Chemistry session Microwave Assisted Synthesis

https://doi.org/10.3390/ecsoc-14-00463

Abstract: The title compound, [6-Diethylamino-9-(2-octylcarbamoyl-phenyl)-xanthen-3-ylidene]-diethyl-amine was synthesized in high yield by an amidation with N-octylamine in a CEM Discover microwave at 60°C for 2 hrs. Its structure was characterized by Ultraviolet-Visible and fluorescence spectral analysis.

Keywords: amidation, microwave

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